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Publications and References

Links

Publications:

  • Arbogast, L.W.; Delaglio, F.; Tolman, J.R.; Marino, J.P.  "Selective Suppression of Excipient Signals in 2D 1H-13C Methyl Spectra of Biopharmaceutical Products" Journal of Biomolecular NMR, 2018,72,149-161. 10.1007/s10858-018-0214-1  PDF

  • Arbogast, L.W.; Delaglio, F.; Brinson, R.G.; Marino, J.P. "Assessment of the Higher Order Structure of Formulated Monoclonal Antibody Therapeutics by 2D Methyl Correlated NMR and Principal Component Analysis"  Current Protocols in Protein Science, 2020, 100, e105.  10.002/cpps.105

References:

Selective Inversion:

  • Tolman, J.; Arbogast, L. "Selective spin inversion in solution by magic field cross polarization" Journal of Magnetic Resonance, 2019, 308, 106588.  10.1016/j.jmr.2019.106588 

  • Arbogast, L.; Majumdar, A.; Tolman, J.  " Unraveling long range dipolar couplings networks in strongly aligned proteins" Journal of Magnetic Resonance, 2013, 235, 26-31.  10.1016/j.jmr.2013.06.024

 

Selective Cross Polarization:

  • Chiarparin, E.; Pelupessy, P.; Bodenhausen, G.  "Selective cross-polarization in solution sate NMR"  Molecular Physics, 1998, 95, 759-767
  • Pelupessy, P.; Chiarparin, E.; Bodenhausen, G. "Excitation of selected proton signals in NMR of isotopically labeled macromolecules"  Journal of Magnetic Resonance, 1999, 138, 178-181.
  • Ferrage, F.; Eykyn, T.R.; Bodenhausen, G. "Coherence transfer by single-transition cross-polarization: Quantization of cross-correlation effects in nuclear magnetic resonance" The Journal of Chemical Physics, 2000, 113,1081-1087.
  • Eykyn, T.R.; Ferrage, F.; Bodenhausen, G. "Hartmann-Han polarization transfer in liquids: An ideal tool for selective experiments"  Concepts in Magnetic Resonance, 2000, 12, 103-124.
  • Eykyn, T.R.; Ferrage, F., Bodenhausen, G. "Quasi-isotropic single-transition cross-polarization in nuclear magnetic resonance"  The Journal of Chemical Physics, 2002, 116, 10041-10050
  • Eykyn, T.R.; Ferrage, F.; Bodenhausen, G. "Highly selective excitation in bimolecular NMR by frequency-switched, single transition cross-polarization"  Journal of the American Chemical Society, 2002, 124, 2076-2077.
  • Eykyn, T.R. Philp, D.J.; Kuchel, P.W.; "Selective cross-polarization in solution state nuclear magnetic resonance of scalar coupled spin 1/2 and quadrupolar nuclei"  The Journal of Chemical Physics, 2003, 118, 6887-7004.
  • Ferrage, F.; Eykyn, T.R.; Bodenhausen, G. "Frequency-switched single-transition cross-polarization: A tool for seletive experiments in biomolecular NMR"  ChemPhysChem, 2003, 5, 76-84.